Efficient Preparation of ortho-Aminobenzenesulfonamides using Ligand-Free Copper(I)-Catalyzed Amination - INRAE - Institut national de recherche pour l’agriculture, l’alimentation et l’environnement
Article Dans Une Revue SYNLETT Année : 2011

Efficient Preparation of ortho-Aminobenzenesulfonamides using Ligand-Free Copper(I)-Catalyzed Amination

Jérôme Thibonnet
Jean-Luc Parrain
Mohamed Abarbri

Résumé

A general and efficient method of copper-catalyzed amination of 2-iodobenzenesulfonamide has been developed under very mild conditions, with good to excellent yields. This method uses inexpensive copper(I) iodide as catalyst, readily available 2-iodobenzenesulfonamides and aliphatic amines as the starting materials, and does not require the use of any ligand system or any expensive supplementary additives.
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Dates et versions

hal-02645591 , version 1 (29-05-2020)

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Zineb Bahlaouan, Jérôme Thibonnet, Alain Duchêne, Jean-Luc Parrain, Mostafa Elhilali, et al.. Efficient Preparation of ortho-Aminobenzenesulfonamides using Ligand-Free Copper(I)-Catalyzed Amination. SYNLETT, 2011, 17, pp.2509 - 2512. ⟨10.1055/s-0030-1260323⟩. ⟨hal-02645591⟩
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