Valorization of industrial wastes from French maritime pine bark by solvent free microwave extraction of volatiles - INRAE - Institut national de recherche pour l’agriculture, l’alimentation et l’environnement Access content directly
Journal Articles Journal of Cleaner Production Year : 2016

Valorization of industrial wastes from French maritime pine bark by solvent free microwave extraction of volatiles

Abstract

Solvent Free Microwave Extraction (SFME) of oil from French maritime pine bark waste and its antioxidant activity were investigated and compared to classical hydrodistillation (HD) method (Clevenger apparatus). A central composite design combined with response surface methodology was applied to evaluate the simultaneous influences of irradiation power and irradiation time. A maximal extraction yield of 3.48% (g/100 g dry bark) was achieved under optimal extraction time of 92.4 min and an irradiation power of 803.5 W compared 2.2% obtained for the conventional method (HD). Gas chromatography coupled to mass spectrometry (GC-MS) analysis showed that SFME extract is richer in oxygenated compounds (~40%) compared to HD extract with 26%. The results also showed that the two independent variables had a statistical significant effect on the considered responses namely oil yield, total phenolic compounds (TPC) and antioxidant activity assessed by 2,2-diphenyl-1-picrylhdrazyl (DPPH). Under optimized conditions, the amount of TPC was 139.15 mg GAE/g extract largely higher than that obtained for HD extraction (14.28 15 mg GAE/g extract) suggesting that SFME represents an interesting alternative technology for production of recoverable oil from waste of French Maritime pine bark. The percentage inhibition was also higher for SFME extraction technique (71.91%) than for HD (56.51%) indicating a higher antioxidant activity.
Fichier principal
Vignette du fichier
2016 - Publi 02 - Mellemiestre_1.pdf (1.31 Mo) Télécharger le fichier
Origin Files produced by the author(s)
Loading...

Dates and versions

hal-02637301 , version 1 (27-05-2020)

Identifiers

Cite

Hamid Mellouk, Alice Meullemiestre, Zoulikha Maache-Rezzoug, Bouchra Bejjani, Adil Dani, et al.. Valorization of industrial wastes from French maritime pine bark by solvent free microwave extraction of volatiles. Journal of Cleaner Production, 2016, 112, pp.4398_4405. ⟨10.1016/j.jclepro.2015.06.129⟩. ⟨hal-02637301⟩
16 View
118 Download

Altmetric

Share

Gmail Mastodon Facebook X LinkedIn More